岩土力学 ›› 2025, Vol. 46 ›› Issue (12): 3841-3854.doi: 10.16285/j.rsm.2025.0008CSTR: 32223.14.j.rsm.2025.0008

• 基础理论与实验研究 • 上一篇    下一篇

基于纳米压痕的岩石矿物微观力学特性研究

易书帆1,张雅慧1,李长冬1, 2,李子繁1,曾凡军1   

  1. 1. 中国地质大学(武汉)工程学院,湖北 武汉 430074;2. 中国地质大学(武汉)湖北巴东地质灾害国家野外科学观测研究站,湖北 武汉 430074
  • 收稿日期:2025-01-03 接受日期:2025-03-20 出版日期:2025-12-11 发布日期:2025-12-15
  • 通讯作者: 张雅慧,女,1994年生,博士,教授,主要从事岩土体灾变细宏观机理方面的研究。E-mail: zhangyahui@cug.edu.cn
  • 作者简介:易书帆,女,2000年生,硕士研究生,主要从事岩石微宏观力学特性方面的研究。E-mail: yishufan@cug.edu.cn
  • 基金资助:
    国家自然科学基金(No.42307223,No.42090054)。

Micromechanical properties of key rock-forming minerals based on nanoindentation

YI Shu-fan1, ZHANG Ya-hui1, LI Chang-dong1, LI Zi-fan1, ZENG Fan-jun1   

  1. 1. Faculty of Engineering, China University of Geosciences, Wuhan, Hubei 430074, China; 2. Badong National Observation and Research Station of Geohazards, China University of Geosciences, Wuhan, Hubei 430074, China
  • Received:2025-01-03 Accepted:2025-03-20 Online:2025-12-11 Published:2025-12-15
  • Supported by:
    This work was supported by the National Natural Science Foundation of China (42307223, 42090054).

摘要: 室内试验是获取岩石力学性质最直接准确的方式。矿物−岩石多尺度分析技术通过数字岩心建模与离散元模拟,揭示了微观矿物力学参数对宏观工程响应的调控机制,为地质灾害防控评估提供了理论工具。纳米压痕试验作为一种研究材料微观力学的重要试验手段,目前对于岩石材料的研究主要集中于页岩、花岗岩,少有关于玄武岩、片麻岩、片岩、板岩等岩石的研究,而更鲜有对于同一造岩矿物在不同岩石中所表现出不同微观力学特性的研究。通过采用粉晶X射线衍射、光学显微镜观察、电子探针、纳米压痕等试验手段,获取了10种岩石中主要造岩矿物的成分、含量、表观形貌及矿物尺度的微观力学特性,针对不同矿物在纳米压痕试验下峰值荷载试验参数的选择,结合大量纳米压痕试验相关文献,将同一矿物在不同岩石中所表现出的微观力学特性差异进行对比并进一步分析原因。结果表明:(1)对压痕试验结果进行拟合,发现断裂韧度与弹性模量间呈显著的线性相关,与硬度间的相关性不显著;(2)石英、钾长石、斜长石合适的峰值荷载为7 mN,云母为3 mN,方解石和白云石为4 mN;(3)不同矿物在纳米压痕中的曲线差异较大,其中石英的试验数据集中性最强,钾长石次之,斜长石、白云石、方解石的数据结果具有一定程度的离散性,云母的数据因其独特的片状结构而离散性最大;(4)将研究中10种岩石的试验数据与他人文献进行对比验证,发现花岗岩的试验数据具有较强的一致性,而其余岩石的研究成果可为纳米压痕试验参数选择提供参考,进一步为岩石从微观力学特性的角度进行参数化建模提供依据,对岩石微宏观力学行为的研究具有重要意义。此外,结合环境地质与可持续开发需求,多尺度分析技术可揭示矿物−岩石在复杂环境下的力学响应机制,进一步拓展了其在新能源材料开发与生态修复工程中的应用前景。

关键词: 岩石矿物, 矿物组分, 纳米压痕试验, 微观力学特性

Abstract: Laboratory testing has become the most direct and accurate method for determining the mechanical properties of rocks. The mineral-rock multiscale analysis technology, using digital core modeling and discrete element simulation, reveals the regulatory mechanism of microscopic mineral mechanical parameters on macroscopic engineering responses, providing a theoretical tool for the assessment and prevention of geological disasters. Nanoindentation is an important technique for studying micromechanics, and current nanoindentation studies on rocks focus mainly on shale and granite; few studies address basalt, gneiss, schist, slate, or other rocks, and little is known about whether the same rock-forming mineral exhibits different micromechanical properties across rocks. In this study, the compositions, contents, apparent morphology and micromechanical properties of the main rock-forming minerals in ten categories of rocks are obtained by means of powder X-ray diffraction test, optical microscope surface observation, electron probe test and nanoindentation test, and the suitable peak loads of different rock-forming minerals for nanoindentation test are selected experimentally. A large body of literature on nanoindentation is compiled to compare the micromechanical properties of the same mineral across rocks and to reveal underlying causes. The indentation results indicate a significant linear relationship between fracture toughness and the elastic modulus; the relationship with hardness is not statistically significant. The appropriate peak load for quartz, potassium feldspar and plagioclase is 7 mN, that for mica is 3 mN, and that for calcite and dolomite is 4 mN. Nanoindentation curves differ substantially among minerals. Quartz data show the least dispersion, followed by potassium feldspar; plagioclase, dolomite, and calcite exhibit moderate dispersion. Compared with published studies, the granite data show strong concordance; for other rocks, the results can guide the selection of nanoindentation parameters. This further provides a basis for parametric modeling of rocks from the perspective of micro-mechanical properties, which is of great significance for studying the micro-macro mechanical behavior of rocks. In addition, in combination with environmental geology and sustainable development needs, multi-scale analysis technology can reveal the mechanical response mechanism of minerals and rocks in complex environments, further expanding its application prospects in the development of new energy materials and ecological restoration engineering.

Key words: rock-forming minerals, mineral components, nanoindentation test, micromechanical properties

中图分类号: TU452
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[3] 刘 笋,蒋明镜,付 昌,朱俊高,. 结构性砂土静力触探试验离散元分析[J]. , 2018, 39(3): 933-942.
[4] 蒋明镜 ,付 昌 ,贺 洁 ,申志福 ,朱方园 , . 不同开采方法下深海能源土离散元模拟[J]. , 2015, 36(S2): 639-647.
[5] 蒋明镜 ,付 昌 ,刘静德 ,李 涛 , . 各向异性结构性砂土离散元分析[J]. , 2015, 36(S1): 577-584.
[6] 罗 荣,曾亚武. 岩石矿物细胞元随机性参数赋值方法研究[J]. , 2012, 33(7): 2221-2228.
[7] 李 萍 ,邓金根 ,孙 焱 ,闫新江 ,徐显广. 川东气田盐岩、膏盐岩蠕变特性试验研究[J]. , 2012, 33(2): 444-448.
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